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Product Details
| Product Name | 2-Methylpiperazine |
| Alias | 2-Methylpiperazine |
| English | |
| Molecular formula | C5H12N2 |
| Molecular weight | 100.16 |
| CAS No | 109-07-9 |
| EINECS | 203-644-2 |
| Specification | Appearance: white to pale yellow crystals Assay: 99.0%min EDA: 0.50%max Water:0.50%max |
| Appearance traits | Pharmaceutical intermediate of the API such as lomefloxacin, Gatifloxacin |
| Use | |
| Package | 50KG/iron drum |
| Other product information | Hazard:UN 2925 4.1/PG 2 HS CODE:2933599090 Molecular Structure:
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Purification Methods |
Purify it by zone melting and by distillation. It is hygroscopic. The picrate has m 275-276o. [Beilstein 23 II 16, 23 III/IV 393, 23/3 V 267.] |
InChI:InChI=1/C10H20N2O2/c1-8-7-11-5-6-12(8)9(13)14-10(2,3)4/h8,11H,5-7H2,1-4H3
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glycerol


piperazine


N-(1-aminomethyl-2-hydroxyethyl)amine


1,2,3-triaminopropane


(RS)-2-methylpiperazine


ethylenediamine


1,2-diaminopropan


3,5-dimethylpiperazine
| Conditions | Yield |
|---|---|
|
With ammonia; hydrogen; Raney nickel; In water; at 200 ℃; under 15001.5 - 150015 Torr; Product distribution / selectivity; Autoclave;
|

glycerol


2-Amino-1-propanol


N-(1-aminomethyl-2-hydroxyethyl)amine


1,2,3-triaminopropane


(RS)-2-methylpiperazine


1,2-diaminopropan


3,5-dimethylpiperazine


2,5-dimethylpiperazine
| Conditions | Yield |
|---|---|
|
With ammonia; hydrogen; catalyst precursor whose active composition comprised 13% by weight of Cu, calculated as CuO, 28% by weight of Ni, calculated as NiO, 28% by weight of Co, calculated as CoO and 31% by weight of Zr, calculated as ZrO2; In water; at 180 ℃; for 53h; under 150015 Torr; Product distribution / selectivity;
|

2-Methylpyrazine

Glyoxal

1,2-diaminopropan

propylene glycol

2-(3-methyl-piperazino)-1,1-diphenyl-ethanol

3-Methyl-piperazin-1-dithiocarbonsaeure

4-(3-methyl-piperazino)-butan-1-ol

3-methylpiperazine-1-carboxylic acid ethyl ester
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