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Product Details
Product Name | 2-Methylpiperazine |
Alias | 2-Methylpiperazine |
English | |
Molecular formula | C5H12N2 |
Molecular weight | 100.16 |
CAS No | 109-07-9 |
EINECS | 203-644-2 |
Specification | Appearance: white to pale yellow crystals Assay: 99.0%min EDA: 0.50%max Water:0.50%max |
Appearance traits | Pharmaceutical intermediate of the API such as lomefloxacin, Gatifloxacin |
Use | |
Package | 50KG/iron drum |
Other product information | Hazard:UN 2925 4.1/PG 2 HS CODE:2933599090 Molecular Structure: |
Purification Methods |
Purify it by zone melting and by distillation. It is hygroscopic. The picrate has m 275-276o. [Beilstein 23 II 16, 23 III/IV 393, 23/3 V 267.] |
InChI:InChI=1/C10H20N2O2/c1-8-7-11-5-6-12(8)9(13)14-10(2,3)4/h8,11H,5-7H2,1-4H3
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glycerol
piperazine
N-(1-aminomethyl-2-hydroxyethyl)amine
1,2,3-triaminopropane
(RS)-2-methylpiperazine
ethylenediamine
1,2-diaminopropan
3,5-dimethylpiperazine
Conditions | Yield |
---|---|
With ammonia; hydrogen; Raney nickel; In water; at 200 ℃; under 15001.5 - 150015 Torr; Product distribution / selectivity; Autoclave;
|
glycerol
2-Amino-1-propanol
N-(1-aminomethyl-2-hydroxyethyl)amine
1,2,3-triaminopropane
(RS)-2-methylpiperazine
1,2-diaminopropan
3,5-dimethylpiperazine
2,5-dimethylpiperazine
Conditions | Yield |
---|---|
With ammonia; hydrogen; catalyst precursor whose active composition comprised 13% by weight of Cu, calculated as CuO, 28% by weight of Ni, calculated as NiO, 28% by weight of Co, calculated as CoO and 31% by weight of Zr, calculated as ZrO2; In water; at 180 ℃; for 53h; under 150015 Torr; Product distribution / selectivity;
|
2-Methylpyrazine
Glyoxal
1,2-diaminopropan
propylene glycol
2-(3-methyl-piperazino)-1,1-diphenyl-ethanol
3-Methyl-piperazin-1-dithiocarbonsaeure
4-(3-methyl-piperazino)-butan-1-ol
3-methylpiperazine-1-carboxylic acid ethyl ester
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