Product Details
General Description |
Hexylphosphonic acid(HPA) is a phosphonic acid derivative that can be used as a capping agent and a surfactant. |
InChI:InChI=1/C6H15O3P/c1-2-3-4-5-6-10(7,8)9/h2-6H2,1H3,(H2,7,8,9)/p-2
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Long-chain n-Alkylphosphonic acids, AlkP...
The invention belongs to the technical f...
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1-bromo-hexane
triethyl phosphite
n-hexylphosphonic acid
Conditions | Yield |
---|---|
1-bromo-hexane; triethyl phosphite; at 150 ℃; for 5h; Large scale;
With hydrogenchloride; In water; at 60 ℃; for 10h; Large scale;
|
170 kg |
1-bromo-hexane
n-hexylphosphonic acid
Conditions | Yield |
---|---|
1-bromo-hexane; With potassium hydroxide semihydrate; phosphorus; cetyltrimethylammonim bromide; In water; toluene; at 85 - 90 ℃; for 6h; Inert atmosphere;
With nitric acid; In water; at 100 - 110 ℃; for 2h; pH=4; Inert atmosphere;
|
61% |
Multi-step reaction with 2 steps
1: heptane
2: concentrated aqueous HCl
With hydrogenchloride; n-heptane;
|
|
Multi-step reaction with 2 steps
1: 15 h / 150 °C / Inert atmosphere
2: trimethylsilyl bromide / dichloromethane; methanol / 20 °C / Inert atmosphere
With trimethylsilyl bromide; In methanol; dichloromethane;
|
dibutyl hexylphosphonate
1-hexene
hexylphosphonic acid dichloride
Hexyl-phosphonsaeure-dimethylester
1-hexene
hexane
diethyl hexylphosphonate
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